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Instrumental Analysis 1 H-NMR spectra were recorded at 400 MHz using a NMR Bruker Ascend 400 MHz for 1 H, and D 2 O or deuterated-phosphate buffer saline (PBS-d) as solvents

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doi: 10.1056/NEJMoa1405760 76 WallischMLorentzCULakshmananHHSJohnsonJCarrisMRPuyCet al

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